原理:试样用乙腈匀浆提取,提取液经盐析,石墨碳黑、丙氨基固相小柱净化后,用气相色谱质谱仪检测305种农药。质谱图由解卷积(deconvolution)软件经噪音处理、基线漂移的修正和共流出谱峰当中单个化合物的识别等处理后,根据被处理的质谱图和保留时间定性,内标法定量;提取液经乙二胺基- N -丙基(PSA)分散固相萃取净化后,用液相色谱质谱仪检测29种农药,根据选择离子丰度比和保留时间定性,外标法定量。(点击图片查看标准详情)
原理:试样用乙腈匀浆提取,提取液经盐析,石墨碳黑、丙氨基固相小柱净化后,用气相色谱质谱仪检测305种农药。质谱图由解卷积(deconvolution)软件经噪音处理、基线漂移的修正和共流出谱峰当中单个化合物的识别等处理后,根据被处理的质谱图和保留时间定性,内标法定量;提取液经乙二胺基- N -丙基(PSA)分散固相萃取净化后,用液相色谱质谱仪检测29种农药,根据选择离子丰度比和保留时间定性,外标法定量。
水 |
去离子水 |
乙腈 |
色谱纯 |
甲醇 |
色谱纯 |
甲苯 |
色谱纯 |
丙酮 |
色谱纯 |
硫酸镁 |
无水硫酸镁,分析纯 |
干燥器 |
– |
滤膜 |
0.22μm |
乙二胺-N-丙基硅烷化硅胶 |
PSA,40μm,6A |
固相萃取柱 |
石墨碳,容积6mL,填料500mg |
固相萃取柱 |
丙氨基,容积6mL,填枓500mg |
冰箱 |
-18℃ |
马弗炉 |
500℃烘烤 |
容量瓶 |
– |
气相色谱串联质谱仪 |
附电子轰击源(EI),带冷阱的程序升温进样口(PTV),解卷积软件,NIST05质谱库 |
液相色谱串联质谱仪 |
液相色谱-质谱仪,附电喷雾离子源 |
分散机 |
高速分散机,转速不低于20000r/min |
离心机 |
– |
旋转蒸发仪 |
– |
氮吹仪 |
– |
冰箱 |
4℃ |
离心管 |
100ml |
鸡心瓶 |
50ml |
纱布 |
– |
离心管 |
2mL |
氮气 |
– |
气相色谱柱 |
HP-5MS(30m×0.25mmx0.25um)石英毛细管柱或相当者 |
氦气 |
载气,纯度≥99.999% |
液相色谱柱 |
C18柱,3.0μm, 150 mmx2.1 mm |
附录A (资料性附录) 表A.1给出了用气相色谱-质谱仪分析的305种农药的中英文名称.保留时间.总离子流图的峰号、方法检出限和混和标准溶液浓度等信息
氘代毒死蜱 |
dl0 – chlorpyrifbs,285138-81-0,纯度≥95% |
乙酰甲胺磷 |
acephate,30560-19-1,纯度≥95% |
啶虫脒 |
acetamiprid,135410-20-7,纯度≥95% |
乙草胺 |
acetochlor,34256-82-1,纯度≥95% |
氟丙菊酯 |
acrinathrin,101007-06-1,纯度≥95% |
甲草胺 |
alachlor,15972-60-8,纯度≥95% |
艾氏剂 |
aldrin,309-00-2,纯度≥95% |
烯丙菊酯 |
allethrin,584-79-2,纯度≥95% |
二丙烯草胺 |
allidochlor,93-71-0,纯度≥95% |
莠灭净 |
ametryn,834-12-8,纯度≥95% |
杀螨特 I |
aramiteⅠ,纯度≥95% |
杀螨特 Ⅱ |
aramite Ⅱ,纯度≥95% |
莠去津 |
atrazine,1912-24-9,纯度≥95% |
氧环唑 |
azaconazole,60207-31-0,纯度≥95% |
益棉磷 |
azinphos-ethyl,2642-71-9,纯度≥95% |
嘧菌酯 |
azoxystrobin,131860-33-8,纯度≥95% |
苯霜灵 |
benalaxyl,71626-11-4,纯度≥95% |
草除灵 |
benazolin-ethyl,25059-80-7,纯度≥95% |
噁虫威 |
恶虫威,bendiocarb,22781-23-3,纯度≥95% |
乙丁氟灵 |
benfluralin,1861-40-1,纯度≥95% |
呋草黄 |
benfuresate,68505-69-1,纯度≥95% |
解草嗪 |
benoxacor,98730-04-2,纯度≥95% |
甲羧除草醚 |
bifenox,42576-02-3,纯度≥95% |
联苯菊酯 |
bifenthrin,82657-04-3,纯度≥95% |
联苯三唑醇I |
bitertanol I,纯度≥95% |
联苯三唑醇 Ⅱ |
bitertanol Ⅱ,纯度≥95% |
除草定 |
bromacil,314-40-9,纯度≥95% |
溴丁酰草胺 |
bromobutide,74712-19-9,纯度≥95% |
溴硫磷 |
bromophos,2104-96-3,纯度≥95% |
乙基溴硫磷 |
bromophos-ethyl,4824-78-6,纯度≥95% |
溴螨酯 |
bromopropylate,18181-80-1,纯度≥95% |
乙嘧酚磺酸酯 |
bupirimate,41483-43-6,纯度≥95% |
噻嗪酮 |
buprofezin,69327-76-0,纯度≥95% |
丁草胺 |
butachlor,23184-66-9,纯度≥95% |
氟丙嘧草酯 |
butafenacil,134605-64-4,纯度≥95% |
抑草磷 |
butamifos,36335-67-8,纯度≥95% |
仲丁灵 |
butralin,33629-47-9,纯度≥95% |
丁草敌 |
butylate,2008-41-5,纯度≥95% |
硫线磷 |
cadusafos,95465-99-9,纯度≥95% |
苯酮唑 |
cafenstrole,125306-83-4,纯度≥95% |
甲萘威 |
carbaryl,63-25-2,纯度≥95% |
克百威 |
carbofuran,1563-66-2,纯度≥95% |
萎锈灵 |
carboxin,5234-68-4,纯度≥95% |
唑草酮 |
carfentrazone-ethyl,128639-02-1,纯度≥95% |
杀螨醚 |
氯杀螨,chlorbenside,103-17-3,纯度≥95% |
氯炔灵 |
chlodbufam,1967-16-4,纯度≥95% |
杀虫脒 |
chlordimefborm,6164-98-3,纯度≥95% |
氯氧磷 |
chloretboxyfos,54593-83-8,纯度≥95% |
溴虫腈 |
虫螨腈,chlorfenapyr,122453-73-0,纯度≥95% |
杀螨酯 |
chlorfenson,80-33-1,纯度≥95% |
毒虫畏 |
chlorfenvinphos,470-90-6,纯度≥95% |
氯甲硫磷 |
chlormephos,60238-56-4,纯度≥95% |
乙酯杀螨醇 |
chlorobenzilate,510-15-6,纯度≥95% |
氯苯甲醚 |
chloroneb,2675-77-6,纯度≥95% |
氯苯胺灵 |
chlorpropham,101-21-3,纯度≥95% |
毒死蜱 |
chlorpyrifos,2921-88-2,纯度≥95% |
甲基毒死蜱 |
chlorpyrifos-methyl,5598-13-0,纯度≥95% |
氯酞酸甲酯 |
chlorthal-dimethyl,1861-32-1,纯度≥95% |
虫螨磷 |
chlorthiophos,60238-56-4,纯度≥95% |
环庚草醚 |
cinmethylin,87818-31-3,纯度≥95% |
顺式-氯丹 |
cis-chlordane,5103-71-9,纯度≥95% |
反式-氯丹 |
trans-chlordane,5103-74-2,纯度≥95% |
炔草酸 |
clodinafop-propargyl,114420-56-3,纯度≥95% |
异恶草松 |
clomazone,80959-17-7,纯度≥95% |
氯甲酰草胺 |
clomeprop,84496-56-0,纯度≥95% |
解草酯 |
解毒喹,cloquintocet-mexyl,99607-70-2,纯度≥95% |
苯腈磷 |
cyanofenpbos,13067-93-1,纯度≥95% |
杀螟腈 |
cyanophos,2636-26-2,纯度≥95% |
环氟菌胺 |
cyflufenamid,180409-60-3,纯度≥95% |
氟氯氰菊酯 I |
cyfluthrin Ⅰ,纯度≥95% |
氟氯氰菊酯 Ⅱ |
cyfluthrin Ⅱ,纯度≥95% |
氟氯氰菊酯 Ⅲ |
cyfluthrin Ⅲ,纯度≥95% |
氟氯氰菊酯 Ⅳ |
cyfluthrin Ⅳ,纯度≥95% |
氰氟草酯 |
cyhalofop-butyl,122008-85-9,纯度≥95% |
氯氰菊酯 I |
cypennethrin I,纯度≥95% |
氯氰菊酯 Ⅱ |
cypennethrin Ⅱ,纯度≥95% |
氟氯氰菊酯 Ⅲ |
cyfluthrin Ⅲ,纯度≥95% |
氟氯氰菊酯 Ⅳ |
cyfluthrin Ⅳ,纯度≥95% |
环丙唑醇 |
cyproconazole,94361-06-5,纯度≥95% |
嘧菌环胺 |
cyprodinil,121552-61-2,纯度≥95% |
o,pˊ-滴滴滴 |
o,pˊ-DDD,53-19-0,纯度≥95% |
p,p’-滴滴滴 |
p,p’-DDD,72-54-8,纯度≥95% |
o,pˊ-滴滴伊 |
o,p’-DDE,3424-82-6,纯度≥95% |
p,p’-滴滴伊 |
p,p’-DDE,72-55-9,纯度≥95% |
o,pˊ-滴滴涕 |
o,p’-DDT,789-02-6,纯度≥95% |
p,p´-滴滴涕 |
p,p’-DDT,50-29-3,纯度≥95% |
溴氰菊酯 |
detamethrin,52918-63-5,纯度≥95% |
硫赶内吸磷 |
内吸磷S,demeton-s,126-75-0,纯度≥95% |
甲基内吸磷 |
demeton-s-methyl,919-86-8,纯度≥95% |
燕麦敌 I |
di-allate I,纯度≥95% |
燕麦敌 Ⅱ |
di-allate Ⅱ,纯度≥95% |
二嗪磷 |
diazinon,333-41-5,纯度≥95% |
敌草腈 |
dichlobenil,1194-65-6,纯度≥95% |
除线磷 |
dichlofenthion,97-17-6,纯度≥95% |
敌敌畏 |
dichlorvos,62-73-7,纯度≥95% |
苄氯三唑醇 |
diclobutrazol,75736-33-3,纯度≥95% |
禾草灵 |
diclofop-methyl,51338-27-3,纯度≥95% |
氯硝胺 |
dicloran,99-30-9,纯度≥95% |
百治磷 |
dicrotophos,141-66-2,纯度≥95% |
狄氏剂 |
dieldrin,60-57-1,纯度≥95% |
乙霉威 |
diethofencarb,87130-20-9,纯度≥95% |
苯醚甲环唑 I |
difenocoazole I,纯度≥95% |
苯醚甲环唑Ⅱ |
difenocoazole Ⅱ,纯度≥95% |
吡氟酰草胺 |
picolinafen,83164-33-4,纯度≥95% |
哌草丹 |
dimepiperate,61432-55-1,纯度≥95% |
异戊乙净 |
dimethametryn,22936-75-0,纯度≥95% |
二甲吩草胺 |
dimethenamid,87674-68-8,纯度≥95% |
噻节因 |
dimethipin,55290-64-7,纯度≥95% |
乐果 |
dimethoate,60-51-5,纯度≥95% |
甲基毒虫畏 |
dimethylvinphos,67628-93-7,纯度≥95% |
烯唑醇 |
diniconazole,83657-24-3,纯度≥95% |
苯虫醚 I |
diofenolan I,纯度≥95% |
苯虫醚 Ⅱ |
diofenolan Ⅱ,纯度≥95% |
蔬果磷 |
dioxabenzofos,3811-49-2,纯度≥95% |
敌噁磷 |
敌恶磷,dioxathion,78-34-2,纯度≥95% |
双苯酰草胺 |
diphenamid,957-51-7,纯度≥95% |
二苯胺 |
diphenylamine,122-39-4,纯度≥95% |
乙拌磷 |
disulfoton,298-04-4,纯度≥95% |
氟硫草定 |
dithiopyr,97886-45-8,纯度≥95% |
敌瘟磷 |
edifenphos,17109-49-8,纯度≥95% |
硫丹 I |
endosulfan I,959-98-8,纯度≥95% |
硫丹 Ⅱ |
endosulfan Ⅱ,33213-65-9,纯度≥95% |
异狄氏剂 |
endrin,72-20-8,纯度≥95% |
苯硫磷 |
EPN,2104-64-5,纯度≥95% |
氟环唑 |
epoxiconazole,133855-98-8,纯度≥95% |
茵草敌 |
EPTC,759-94-4,纯度≥95% |
戊草丹 |
esprocarb,85785-20-2,纯度≥95% |
乙丁烯氟灵 |
ethalfluralin,55283-68-6,纯度≥95% |
乙硫苯威 |
ethiofencarb,29973-13-5,纯度≥95% |
乙硫磷 |
ethion,563-12-2,纯度≥95% |
乙氧苯草胺 |
ethobenzanid,79540-50-4,纯度≥95% |
乙氧呋草黄 |
乙氧夫草黄,ethofumesate,26225-79-6,纯度≥95% |
灭线磷 |
ethoprophos,13194-48-4,纯度≥95% |
醚菊酯 |
etofenprox,80844-07-1,纯度≥95% |
乙螨唑 |
etoxazole,153233-91-1,纯度≥95% |
土菌灵 |
etridiazde,2593-15-9,纯度≥95% |
乙嘧硫磷 |
etrimfos,38260-54-7,纯度≥95% |
苯线磷 |
fenamiphos,22224-92-6,纯度≥95% |
氯苯嘧啶醇 |
fenarimol,60168-88-9,纯度≥95% |
腈苯唑 |
fenbuconazole,114369-43-6,纯度≥95% |
杀螟硫磷 |
fenitrothion,122-14-5,纯度≥95% |
仲丁威 |
fenobucarb,3766-81-2,纯度≥95% |
苯硫威 |
fenothiocarb,62850-32-2,纯度≥95% |
氰菌胺 |
稻瘟酰胺,fenoxanil,115852-48-7,纯度≥95% |
噁唑禾草灵 |
恶唑禾草灵,fenoxaprop-ethyl,77400-65-8,纯度≥95% |
苯氧威 |
fenoxycarb,72490-01-8,纯度≥95% |
甲氰菊酯 |
fenpropathrin,64257-84-7,纯度≥95% |
丰索磷 |
fensulfothioin,115-90-2,纯度≥95% |
倍硫磷 |
fenthion,55-38-9,纯度≥95% |
氰戊菊酯 I |
fenvalerate I,纯度≥95% |
氰戊菊酯 Ⅱ |
fenvalerate Ⅱ,纯度≥95% |
氟虫腈 |
fipronil,120068-37-3,纯度≥95% |
嘧螨酯 |
fluacrypyrim,229977-93-9,纯度≥95% |
吡氟禾草灵 |
fluazifop butyl,69806-50-4,纯度≥95% |
氟氰戊菊酯 I |
flucythrinate I,纯度≥95% |
氟氰戊菊酯 Ⅱ |
flucythrinate Ⅱ,纯度≥95% |
咯菌腈 |
fludioxonil,131341-86-1,纯度≥95% |
氟烯草酸 |
flumiclorac-pentyl,87546-18-7,纯度≥95% |
丙炔氟草胺 |
flumioxazin,103361-09-7,纯度≥95% |
氟喹唑 |
fluquincnnazole,136426-54-5,纯度≥95% |
氟啶草酮 |
fluridone,59756-60-4,纯度≥95% |
氟硅唑 |
flusilazole,85509-19-9,纯度≥95% |
氟酰胺 |
flutolanil,66332-96-5,纯度≥95% |
粉唑醇 |
flutriafol,76674-21-0,纯度≥95% |
地虫硫磷 |
fonofos,944-22-9,纯度≥95% |
安硫磷 |
formothion,2540-82-1,纯度≥95% |
噻唑磷 I |
fosthiazateⅠ,纯度≥95% |
噻唑磷 Ⅱ |
fosthiazateⅡ,纯度≥95% |
四氯苯酞 |
fthalide,27355-22-2,纯度≥95% |
呋线威 |
furathiocarb,65907-30-4,纯度≥95% |
解草恶唑 |
furilazole,121776-33-8,纯度≥95% |
苄螨醚 |
halfenprox,111872-58-3,纯度≥95% |
七氯 |
haptachlor,76-44-8,纯度≥95% |
环氧七氯 |
heptachlorepoxid,1024-57-3,纯度≥95% |
六氯苯 |
hexachlorobenzene,118-74-1,纯度≥95% |
己唑醇 |
hexaconazole,79983-71-4,纯度≥95% |
噻螨酮 |
hexythiazox,78587-05-0,纯度≥95% |
茚虫威 |
indoxacarb,144171-61-9,纯度≥95% |
碘硫磷 |
iodofenphos,18181-70-9,纯度≥95% |
异稻瘟净 |
iprobenfos,26087-47-8,纯度≥95% |
异菌脲 |
iprodione,36734-19-7,纯度≥95% |
缬霉威 I |
iprovalicarb I,纯度≥95% |
缬霉威 Ⅱ |
iprovalicarb Ⅱ,纯度≥95% |
氯唑磷 |
isazofos,42509-80-8,纯度≥95% |
丁咪酰胺 |
丁脒酰胺,isocarbamid,30979-48-7,纯度≥95% |
水胺硫磷 |
isocarbophos,24353-61-5,纯度≥95% |
异艾氏剂 |
isodrin,465-73-6,纯度≥95% |
异柳磷 |
isofenphos,25311-71-1,纯度≥95% |
异丙威 |
isopiocarb,2631-40-5,纯度≥95% |
稻瘟灵 |
isoprothiolane,50512-35-1,纯度≥95% |
醚菌酯 |
kresoxim-methyl,143390-89-0,纯度≥95% |
乳氟禾草灵 |
lactofen,77501-63-4,纯度≥95% |
高效氯氟氰菊酯 |
三氟氯氰菊酯,lambda-cyhalothrin,91465-08-6,纯度≥95% |
环草啶 |
lenacil,218-499-0,纯度≥95% |
二甲威 |
macbal,2655-14-3,纯度≥95% |
马拉硫磷 |
malathion,121-75-5,纯度≥95% |
灭蚜磷 |
mecarbam,2595-54-2,纯度≥95% |
苯噻酰草胺 |
mefenacet,73250-68-7,纯度≥95% |
灭锈胺 |
mepronil,55814-41-0,纯度≥95% |
甲霜灵 |
metalaxyl,57837-19-1,纯度≥95% |
虫螨畏 |
methacrifos,62610-77-9,纯度≥95% |
甲胺磷 |
methamidophos,10265-92-6,纯度≥95% |
杀扑磷 |
methidathion,950-37-8,纯度≥95% |
甲硫威 |
methiocarb,2032-65-7,纯度≥95% |
灭多威 |
methomyl,16752-77-5,纯度≥95% |
烯虫酯 |
methoprene,40596-69-8,纯度≥95% |
甲氧滴滴涕 |
methoxychlor,72-43-5,纯度≥95% |
异丙甲草胺 |
metolachlor,51218-45-2,纯度≥95% |
苯氧菌胺 |
metominostrobin,133408-50-1,纯度≥95% |
嗪草酮 |
metribuzin,21087-64-9,纯度≥95% |
速灭磷 |
mevinphos,7786-34-7,纯度≥95% |
禾草敌 |
molinate,2212-67-1,纯度≥95% |
久效磷 |
monocrotophos,6923-22-4,纯度≥95% |
腈菌唑 |
myclobutanil,88671-89-0,纯度≥95% |
敌草胺 |
napropamide,15299-99-7,纯度≥95% |
甲磺乐灵 |
nitralin,4726-14-1,纯度≥95% |
三氯甲基吡啶 |
nitrapyrin,1929-82-4,纯度≥95% |
酞菌酯 |
nitrothal-isopropyl,10552-74-6,纯度≥95% |
氟草敏 |
norflurazon,27314-13-2,纯度≥95% |
氧乐果 |
omethoate,1113-02-6,纯度≥95% |
噁草酮 |
恶草酮,oxadiazon,19666-30-9,纯度≥95% |
噁霜灵 |
恶霜灵,oxadixyl,77732-09-3,纯度≥95% |
乙氧氟草醚 |
oxyfluorfen,42874-03-3,纯度≥95% |
多效唑 |
paclcbutrazol,76738-62-0,纯度≥95% |
对氧磷 |
paraoxon,311-45-5,纯度≥95% |
甲基对氧磷 |
paraoxon-methyl,950-35-6,纯度≥95% |
对硫磷 |
parathion,56-38-2,纯度≥95% |
甲基对硫磷 |
parathion-methyl,298-00-0,纯度≥95% |
克草敌 |
pebulate,1114-71-2,纯度≥95% |
戊菌唑 |
penconazole,66246-88-6,纯度≥95% |
戊菌隆 |
pencycuron,66063-05-6,纯度≥95% |
二甲戊灵 |
pendimethalin,40487-42-1,纯度≥95% |
氯菊酯 I |
permethrin I,纯度≥95% |
氯菊酯 Ⅱ |
permethrin Ⅱ,纯度≥95% |
乙滴涕 |
perthane,72-56-0,纯度≥95% |
稻丰散 |
phenthoate,2597-03-7,纯度≥95% |
联苯酚 |
o-phenylphenol,纯度≥95% |
甲拌磷 |
phorate,298-02-2,纯度≥95% |
伏杀硫磷 |
phosalone,2310-17-0,纯度≥95% |
磷胺 I |
phosphamidon I,纯度≥95% |
磷胺 II |
phosphamidon II,纯度≥95% |
吡氟酰草胺 |
diflufenican,83164-33-4,纯度≥95% |
增效醚 |
piperonyl-butoxide,51-03-6,纯度≥95% |
哌草磷 |
piperophos,24151-93-7,纯度≥95% |
抗蚜威 |
pirimicarb,23103-98-2,纯度≥95% |
嘧啶磷 |
pirimiphos-ethyl,23505-41-1,纯度≥95% |
甲基嘧啶磷 |
pirimiphos-methyl,29232-93-7,纯度≥95% |
炔丙菊酯 |
炔酮菊酯,prallethrin,23031-36-9,纯度≥95% |
丙草胺 |
pretilachlor,51218-49-6,纯度≥95% |
咪鲜胺 |
prochloraz,67747-09-5,纯度≥95% |
腐霉利 |
procymidone,32809-16-8,纯度≥95% |
丙溴磷 |
profenofos,41198-08-7,纯度≥95% |
猛杀威 |
promecarb,2631-37-0,纯度≥95% |
扑草净 |
prometryne,7287-19-6,纯度≥95% |
毒草胺 |
propachlor,1918-16-7,纯度≥95% |
霜霉威 |
propamocarb,24579-73-5,纯度≥95% |
敌稗 |
propanil,709-98-8,纯度≥95% |
丙虫磷 |
propaphos,7292-16-2,纯度≥95% |
炔螨特 |
propargite,2312-35-8,纯度≥95% |
扑灭津 |
propazine,139-40-2,纯度≥95% |
胺丙畏 |
propetamphos,31218-83-4,纯度≥95% |
苯胺灵 |
propham,122-42-9,纯度≥95% |
丙环唑 I |
propiconazole Ⅰ,纯度≥95% |
丙环唑 Ⅱ |
propiconazole Ⅱ,纯度≥95% |
残杀威 |
propoxur,114-26-1,纯度≥95% |
炔苯酰草胺 |
propyzamide,23950-58-5,纯度≥95% |
丙硫磷 |
prothiofos,34643-46-4,纯度≥95% |
吡唑硫磷 |
pyraclofos,77458-01-6,纯度≥95% |
吡草醚 |
pyraflufen-ethyl,129630-19-9,纯度≥95% |
吡菌磷 |
pyrazophos,13457-18-6,纯度≥95% |
稗草丹 |
pyributicarb,88678-67-5,纯度≥95% |
哒螨灵 |
pyridaben,96489-71-3,纯度≥95% |
哒嗪硫磷 |
pyridafenthion,119-12-0,纯度≥95% |
啶斑肟 I |
pyrifenoxⅠ,纯度≥95% |
噻斑肟 Ⅱ |
pyrifenoxⅡ,纯度≥95% |
嘧霉胺 |
pyrimethanil,53112-28-0,纯度≥95% |
嘧螨醚 |
PYRIMIDIFEN,105779-78-0,纯度≥95% |
嘧草醚 |
pyriminobac-methyl,136191-64-5,纯度≥95% |
吡丙醚 |
pyriproxyfen,95737-68-1,纯度≥95% |
喹硫磷 |
quinalphos,13593-03-8,纯度≥95% |
灭藻醌 |
quinoclamine,2797-51-5,纯度≥95% |
喹氧灵 |
quinoxyfen,124495-18-7,纯度≥95% |
五氯硝基苯 |
quintozene,82-68-8,纯度≥95% |
精喹禾灵 |
quizalofop-ethyl,100646-51-3 ,纯度≥95% |
苄呋菊酯 |
resmethrin,10453-86-8,纯度≥95% |
皮蝇磷 |
ronnel,299-84-3,纯度≥95% |
西玛津 |
simazine,122-34-9,纯度≥95% |
硅氟唑 |
simeconazole,149508-90-7,纯度≥95% |
西草净 |
simetryn,1014-70-6,纯度≥95% |
氟胺氰菊酯 I |
tau-fluvalinate Ⅰ,纯度≥95% |
氟胺氰菊酯 Ⅱ |
tau-fluvalinate Ⅱ,纯度≥95% |
戊唑醇 |
tebuoonazole,107534-96-3,纯度≥95% |
吡螨胺 |
tebufenpyrad,119168-77-3,纯度≥95% |
四氯硝基苯 |
tecnazene,117-18-0,纯度≥95% |
七氟菊酯 |
tefluthrin,79538-32-2,纯度≥95% |
特普 |
TEPP,107-49-3,纯度≥95% |
特草定 |
terbacil,5902-51-2,纯度≥95% |
特丁硫磷 |
terbufos,13071-79-9,纯度≥95% |
特丁津 |
terbuthylazine,5915-41-3,纯度≥95% |
特丁净 |
terbutryn,886-50-0,纯度≥95% |
杀虫畏 |
tetrachlorvinphos,22248-79-9,纯度≥95% |
四氟醚唑 |
氟醚唑,tetraconazole,112281-77-3,纯度≥95% |
三氯杀螨砜 |
tetradifon,116-29-0,纯度≥95% |
噻吩草胺 |
thenylchlor,96491-05-3,纯度≥95% |
噻唑烟酸 |
thiazopyr,117718-60-2,纯度≥95% |
噻呋酰胺 |
thifluzamide,130000-40-7,纯度≥95% |
禾草丹 |
thiobencarb,28249-77-6,纯度≥95% |
甲基乙拌磷 |
thiometon,640-15-3,纯度≥95% |
甲基立枯磷 |
tolclofos-methyl,57018-04-9,纯度≥95% |
三唑酮 |
triadimefon,43121-43-3,纯度≥95% |
三唑醇 |
triadimenol,55219-65-3,纯度≥95% |
野麦畏 |
triallate,2303-17-5,纯度≥95% |
三唑磷 |
triazophos,24017-47-8,纯度≥95% |
脱叶磷 |
tribufos,78-48-8,纯度≥95% |
敌百虫 |
trichlorfon,52-68-6,纯度≥95% |
三环唑 |
tricyclazole,41814-78-2,纯度≥95% |
灭草环 |
tridiphane,58138-08-2,纯度≥95% |
肟菌酯 |
trifloxystrobin,141517-21-7,纯度≥95% |
氟菌唑 |
triflumizole,68694-11-1,纯度≥95% |
氟乐灵 |
trifluralin,1582-09-8,纯度≥95% |
烯效唑 |
uniconazole,83657-22-1,纯度≥95% |
灭草敌 |
vernolate,1929-77-7,纯度≥95% |
乙烯菌核利 |
vinclozolin,50471-44-8,纯度≥95% |
α-六六六 |
α-BCH,319-84-6,纯度≥95% |
β-六六六 |
β-BCH,319-85-7,纯度≥95% |
γ-六六六 |
γ-BCH,58-89-9,纯度≥95% |
δ-六六六 |
δ-BCH,319-86-8,纯度≥95% |
阿维菌素 |
Abamectin,71751-41-2 |
杀草强 |
Amitrole,61-82-5 |
丙硫克百威 |
Benfuracarb,82560-54-1 |
苄嘧磺隆 |
Bensulfuron-methyl,83055-99-6 |
溴敌隆 Ⅰ |
– |
溴敌隆 Ⅱ |
– |
丁硫克百威 |
Carbosulfan,55285-14-8 |
灭幼脲 |
Chlorobenzuron,57160-47-1 |
氟啶脲 |
Chlorfluazuron,71422-67-8 |
氯嘧磺隆 |
Chlorimuron-ethyl,90982-32-4 |
氯磺隆 |
Chlorsulfuron,64902-72-3 |
霜脲氰 |
cymoxanil,57966-95-7 |
烯酰吗啉 Ⅰ |
dimethomorph Ⅰ,110488-70-5 |
烯酰吗啉 Ⅱ |
dimethomorph Ⅱ |
敌草隆 |
diuron,330-54-1 |
唑螨酯 |
fenpyroximate,134098-61-6 |
氟虫脲 |
flufenoxuron,101463-69-8 |
氟铃脲 |
hexaflumuron,86479-06-3 |
噁霉灵 |
恶霉灵,hymexazol,10004-44-1 |
吡虫啉 |
imidacloprid,138261-41-3 |
利谷隆 |
Linuron,330-55-2 |
虱螨脲 |
lufenuron,103055-07-8 |
甲氧虫酰肼 |
methoxyfenozide,161050-58-4 |
甲磺隆 |
Metsulfuron-methyl,74223-64-6 |
灭草隆 |
monuron,150-68-5 |
氨磺乐灵 |
oryzalin,19044-88-3 |
辛硫磷 |
phoxim,14816-18-3 |
多杀菌素 Ⅰ |
spinosad Ⅰ,168316-95-8 |
多杀菌素 Ⅱ |
spinosad Ⅱ |
虫酰肼 |
tebufenozide,112410-23-8 |
氟苯脲 |
teflubenzuron,83121-18-0 |
噻虫嗪 |
thiamethoxam,153719-23-4 |
评论前必须登录!
立即登录 注册